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We want to thank KNTEC for their financial support.
Korean Delegates and invited guests
Chair : O. Karis
In 2016, MAX IV inaugurated the first fourth-generation storage ring in the world. With unprecedented performance, this new accelerator paved the way for a new era of X-ray science. Currently, four more fourth-generation light sources are in operation, with many more to come online by 2040. Overall, the accelerator community is making considerable advancements in Multi-Bend Achromat (MBA)-type lattices. This is to such an extent that, whereas MAX IV paved the way for fourth-generation light sources, we will have difficulties competing with other synchrotrons in the future.
With this in mind, we developed our vision for the laboratory to ensure the excellence, relevance, and leadership of Swedish academic and industrial research with X-rays for the next decades.
This is called MAX 4U, and is our proposal to upgrade our 3GeV storage ring [1]. MAX 4U will reduce the 3GeV ring horizontal emittance further from the current of 328pm×rad to better than 100pm×rad on the horizon of the early 2030s. Beyond an accelerator upgrade, MAX 4U provides opportunities for beamline performance improvements that will keep MAX IV a leading platform for accelerating science, discovery, and innovation.
[1] https://maxiv.lu.se/max4u
When X-ray microscopy results are reported a high amount of consideration is given the metric of resolution. Not a single result can be published without indicating the smallest feature size that can be resolved. With a pursuit for resolving ever smaller, and thus thinner, features another metric becomes more and more important, but is so far rarely reported [1,2] : sensitivity, the capability to distinguish between tiny differences in the signal strength.
In the presented work we explore the limits of how little signal can be detected with current setups and approaches. As the demonstration example we chose the hard X-ray ptychographic dichroic signal from 1μm thick Fe/Gd films [3,4] recorded at the NanoMAX beamline [5,6] at MAX IV. The very specific sample was chosen, because the electronic contribution of the homogeneous sample thickness cancels out and the magnetic signal can be arbitrarily small when tuning the probing beams photon energy.
We reliably recovered signals below 1 mrad in relative phase shift, the smallest signals recovered via ptychography reported to date.
Acknowledgments
We acknowledge the MAX IV Laboratory for beamtime on the NanoMAX beamline under proposal 20240988. Research conducted at MAX IV, a Swedish national user facility, is supported by Vetenskapsrådet (Swedish Research Council, VR) under contract 2018-07152, Vinnova (Swedish Governmental Agency for Innovation Systems) under contract 2018-04969 and Formas under contract 2019-02496.
References
[1] Y. Takahashi et al. J. Synchrotron Rad. 30, 989–994 (2023)
[2] N. Okawa et al. Microscopy and Microanalysis 30.5 836-843 (2024)
[3] C. Donnelly et al. Phys. Rev. B 94, 06442 (2016)
[4] J. Neethirajan et al. Phys. Rev. X 14, 031028 (2024)
[5] D. Carbone et al. J. Synchrotron Rad. 29, 876-887 (2022)
[6] U. Johansson et al. J. Synchrotron Rad. 28, 1935-1947 (2021)
Korean Delegates, Speakers, and Guests
MAX IV operates a suite of instruments dedicated to X-ray spectroscopy, several of which offer advanced operando and in-situ methods to study materials under operational conditions. Specifically, on the 3 GeV ring, the worlds first operational 4th generation synchrotron light source, the HIPPIE beamline provides extensive state-of-the-art ambient pressure photoelectron spectroscopy instrumentation.
This talk will overview our latest developments, focussing on time resolved methods to probe reaction kinetics and new sample environments that unlock new possibilities. Highlights will include a new reaction cell allowing measurements at high temperatures with inbuilt valves for controlling gas flow, our first studies in plasma environments, a demonstration of APXPS combined with IR spectroscopy, and our first steps in the direction of time-resolved electrochemical APXPS.